2006-12-04, English, Article, Journal or magazine article edition: A comparative study of reactive direct current magnetron sputtered CrAlN and CrN coatings. Barshilia, Harish C.; Selvakumar, N.; Deepthi, B.; ...

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Physical Description
  • Magazine/​Journal article
Published
  • Elsevier B.V., 2006 Dec 4
Language
  • English

Edition details

Title
  • A comparative study of reactive direct current magnetron sputtered CrAlN and CrN coatings.
Appears In
  • Surface &​ Coatings Technology, v.201, no.6, 2006 Dec 4, p.2193(9) (ISSN: 0257-8972)
Author
  • Barshilia, Harish C.
  • Selvakumar, N.
  • Deepthi, B.
  • Rajam, K.S.
Published
  • Elsevier B.V., 2006 Dec 4
Physical Description
  • Magazine/​Journal article
Subjects
Target Audience
  • Academic
Summary
  • To link to full-text access for this article, visit this link: http:/​/​dx.doi.org/​10.1016/​j.surfcoat.2006.03.037 Byline: Harish C. Barshilia, N. Selvakumar, B. Deepthi, K.S. Rajam Keywords: CrN and CrAlN coatings; Magnetron sputtering; Structure and mechanical properties; Thermal stability; Surface roughness; Corrosion resistance Abstract: Approximately 1.5 [mu]m thick CrN and CrAlN coatings were deposited on silicon and mild steel substrates by reactive direct current (DC) magnetron sputtering. The structural and mechanical properties of the coatings were characterized using X-ray diffraction (XRD) and nanoindentation techniques, respectively. The bonding structure of the coatings was characterized by X-ray photoelectron spectroscopy (XPS). The surface morphology of the coatings was studied using scanning electron microscopy (SEM) and atomic force microscopy (AFM). The XRD data showed that the CrN and CrAlN coatings exhibited B1 NaCl structure. Nanoindentation measurements showed that as-deposited CrN and CrAlN coatings exhibited a hardness of 18 and 33 GPa, respectively. Results of the surface analysis of the as-deposited coatings using SEM and AFM showed a more compact and dense microstructure for CrAlN coatings. The thermal stability of the coatings was studied by heating the coatings in air from 400 to 900 [degrees]C. The structural changes as a result of heating were studied using micro-Raman spectroscopy. The Raman data revealed that CrN coatings got oxidized at 600 [degrees]C, whereas in the case of CrAlN coatings, no detectable oxides were formed even at 800 [degrees]C. After annealing up to 700 [degrees]C, the CrN coatings displayed a hardness of only about 7.5 GPa as compared to CrAlN coatings, which exhibited hardness as high as 22.5 GPa. The potentiodynamic polarization measurements in 3.5% NaCl solution indicated that the CrAlN coatings exhibited superior corrosion resistance as compared to CrN coatings. Author Affiliation: Surface Engineering Division, National Aerospace Laboratories, Post Bag No. 1779, Bangalore - 560 017, India Article History: Received 17 February 2006; Accepted 21 March 2006
Terms of Use
  • COPYRIGHT 2006 Elsevier B.V.
Language
  • English
Database
  • Gale Academic OneFile
Identifier
  • 196090317

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