English, Article edition: SYNTHESIS, AND SURFACE-ACTIVE PROPERTIES OF PALM FATTY ACID AND 1(2-HYDROXYETHYL PIPERAZINE)-BASED ESTERAMIDE QUAT SHILPI MISHRA; V. K. TYAGI

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Bookmark: http://trove.nla.gov.au/version/84156
Physical Description
  • article
Language
  • English

Edition details

Title
  • SYNTHESIS, AND SURFACE-ACTIVE PROPERTIES OF PALM FATTY ACID AND 1(2-HYDROXYETHYL PIPERAZINE)-BASED ESTERAMIDE QUAT
Author
  • SHILPI MISHRA
  • V. K. TYAGI
Physical Description
  • article
Notes
  • In this study, an attempt has been made to synthesize esteramide quat by esterification of palm fatty acids with 1(2-hydroxyethyl piperazine) followed by quaternization with dimethyl sulphate (DMS). The optimum reaction conditions for esterification of palm fatty acids and 1(2-hydroxyethyl piperazine) were found to be 170°C reaction temperature and 150 mmHg pressure. The obtained esteramide was subjected to quaternization with different molar ratios of DMS. The consequences revealed that esteramide to DMS ratio of 1 : 0.95 and duration of quaternization for 2 h yielded esteramide quat of maximum cationic content, i.e., 64.9%. The instrumental analysis, viz. FT-IR, 1H NMR, 13C NMR verified the esterification and subsequent quaternization of the obtained esteramide quat. Furthermore, the surface-active and performance properties of synthesized esteramide quat were also evaluated.
  • Esteramide quat, esterification, quaternization, softness, rewettability, surface tension, cationic content
  • RePEc:wsi:srlxxx:v:14:y:2007:i:06:p:1129-1133
Language
  • English
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